Oil Bath Assembly
Mineral oil or silicone oil is typically used for oil baths in research labs for reactions that require heating/reflux temperatures up to 200 °C. Oil baths provide more uniform heat in comparison to other heating devices. A laboratory oil bath is made of an aluminum or stainless steel pan, a heavy porcelain dish or thick walled Pyrex® glass to withstand breakage and accidental spill.
Oil bath and heating mandle The electric heating coil (or oil bath on a hot plate) is controlled using a variable voltage controller (i.e., Variac). The voltage controller is adjusted to increase or decrease the temperature setting of the oil bath. Heating mantles should NEVER be plugged directly into an outlet. Comparison of Heating Assemblies Bath Material Useful Range Flash Point Advantage/Disadvantage Risk Silicone Oil 25 °C to 230 °C 150 °C to 350 °C Chemically inert to organic materials. Easy to clean up and reuse. Does not degrade. Can be used with a glass wool support in a heating mantle or metal container with a Variac that provides uniform heat distribution. Spatter danger much lower. Warning: DO NOT let the distillation flask become dry while using a sand bath for vacuum distillation. (At high temperatures and vacuum, a dry glass flask can become soft and implode.) LOW Personal Protective Equipment (PPE) Slip-resistant insulated thermal gloves. Safety glasses with side shields or a face shield. Lab coat Appropriate clothing should always be worn in the laboratory which includes closed-toe shoes and long pants/skirt. Prudent Safety Practices Do not place a flat-bottom Pyrex glass oil bath directly on a stirring/hot plate, as this is a fire hazard. Oil baths prepared with Pyrex glass should be placed within a metal secondary container to prevent the glass from breaking and spilling the hot oil. The desired oil temperature MUST BE lower than the flash point of the oil. Avoid overheating the oil bath. Smoke indicates that the current temperature is above the safe operating range and smoking oil is highly susceptible to ignition. Do not exceed the recommended temperature limits of the oil. Discard oil that was overheated or appears dark brown in color. The oil bath must be monitored using a thermometer. For unattended reactions, oil baths should be fitted with a temperature monitoring device and timer/automatic shut off for the heating operation. This must be set to maintain the heat well below the flash point of the oil. Do not overfill the oil bath. Safe depth for an oil bath is no more than two-thirds of the container height when the reaction flask is immersed in the oil. Use thick–walled, round-bottom flasks in oil baths for reflux or distillation reactions. Clamp the reaction flask at a safe bath height with an adjustable clamp. If the reaction begins to overheat, the bath height can be immediately adjusted and replaced with a cooling bath. Make sure to prevent water from leaking into hot oil baths, which can cause the oil to pop and splatter. In the event of fire, do not use water to put it out. Storage
Store the oil bath away from heat sources, including hot plates. When not in use, keep the oil bath covered with a metal cover or cover the bath container with aluminum foil, and store at room temperature. Before storing, label the bath with the contents of the oil (fluid name) as well as with the safe working temperature range of the fluid. Do not store used oil, including oil drained from the vacuum pump, in any open container including plastic buckets, or rectangular sharps or Biohazard containers.
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